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and then themixture w as high-energy ball milling during 30h in a planetary ball mill (Fritsch Pulverisette 5). The rotation speed of the disks carrying the sealed vials was 370 rpm. This operation was used to improve the homogeneity of the powder. Then the powder was calcined at 1050 C for 12h. X-ray diffraction The X-ray powder diffraction profiles of the samples were
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Planetary Mills are ideally suited for fine grinding of hard, medium-hard, soft, brittle, tough and moist materials. The comminution of the material to be ground takes place primarily through the high-energy impact of grinding balls in rotating grinding bowls. The grinding can be performed dry, in suspension or in inert gas.
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